Methyl 4-Hydroxycyclohexanecarboxylate
methyl 4-hydroxycyclohexanecarboxylate
CAS: 17449-76-2
Molecular Formula: C8H14O3
Methyl 4-Hydroxycyclohexanecarboxylate - Names and Identifiers
Methyl 4-Hydroxycyclohexanecarboxylate - Physico-chemical Properties
| Molecular Formula | C8H14O3 |
| Molar Mass | 158.2 |
| Density | 1.121 |
| Boling Point | 233℃ |
| Flash Point | 94℃ |
| Vapor Presure | 8.14E-06mmHg at 25°C |
| pKa | 14.96±0.40(Predicted) |
| Storage Condition | Sealed in dry,Room Temperature |
| Refractive Index | 1.681 |
Methyl 4-Hydroxycyclohexanecarboxylate - Reference Information
| Introduction | Methyl 4-hydroxycyclohexanecarboxylate is an organic intermediate, which can be obtained by esterification of 4-hydroxycyclohexanoic acid or obtained by reduction of methyl 4-oxocyclohexanecarboxylic acid. |
| Preparation | The methanol (30mL) suspension of stirred 4-hydroxycyclohexane-1-carboxylic acid (SM-1)(15g,104.1mmol) was dropwise added with sulfuric acid (0.9mL,15.6mmol) at room temperature in a nitrogen atmosphere and stirred at RT for 5 hours. After feedstock consumption (TLC monitoring), the reaction was quenched with water (50mL) and extracted with EtOAc (2x 100mL). The combined organic layer was washed with saturated NaHCO3 solution and saline solution. The organic layer is dried and concentrated under reduced pressure on Na2SO4 to provide methyl 4-hydroxycyclohexanarate (13.5g,82%), which is a liquid. |
Last Update：2024-04-10 22:29:15
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View History
Methyl 4-Hydroxycyclohexanecarboxylate
三氟(2-甲基丙-1-烯-1-基)硼酸钾
Tricyclo[4.4.0.0(2,7)]dec-3-ene, 1,3-dimethyl-8-(1-methylethyl)-, st
血管活性肠肽(VIP)检测试剂盒( ELISA 方法)
2-{[2-(difluoromethoxy)phenyl]carbonyl}-N-(4-ethylphenyl)hydrazinecarbothioamide
Dimethylmalonic acid bis[2-(2-ethoxyethoxy)ethyl] ester
tert-Butyl 4-fluoro-3-(hydroxymethyl)piperidine-1- carboxylate...
Lacidipine Solution, 100ppm
(S)-2-氨基-4-环己基丁酸
三氟(2-甲基丙-1-烯-1-基)硼酸钾
Tricyclo[4.4.0.0(2,7)]dec-3-ene, 1,3-dimethyl-8-(1-methylethyl)-, st
血管活性肠肽(VIP)检测试剂盒( ELISA 方法)
2-{[2-(difluoromethoxy)phenyl]carbonyl}-N-(4-ethylphenyl)hydrazinecarbothioamide
Dimethylmalonic acid bis[2-(2-ethoxyethoxy)ethyl] ester
tert-Butyl 4-fluoro-3-(hydroxymethyl)piperidine-1- carboxylate...
Lacidipine Solution, 100ppm
(S)-2-氨基-4-环己基丁酸